X-ray computed tomography

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Connect results with scale and specimen preparation.

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Focused ion beam SEM

A scanning electron microscope paired with an ion beam that mills material away at a chosen spot. It cuts clean cross-sections through particles and coatings, lifts out thin slices for TEM, and by alternately milling and imaging rebuilds an electrode’s microstructure in 3D for porosity and tortuosity.

Jelly roll

Electrodes and separators wound together into a spiral. It is the inside of a cylindrical cell and of many prismatic cells; large pouch cells usually use stacked sheets instead.

Porosity

The fraction of a layer’s volume that is empty space. In a lithium-ion electrode the pores — roughly 20–35 % of the volume after calendering — are filled with electrolyte, which carries ions to the particles.

Post-mortem analysis

Opening an aged or failed cell in an inert glovebox and examining its electrodes by microscopy, diffraction and chemical analysis. It confirms which degradation mechanisms actually occurred rather than inferring them from voltage.

Thermal runaway

Self-accelerating heating in a cell: heat speeds up reactions that release more heat, until the cell vents, catches fire or ruptures. An internal short, overcharge or external heating can trigger it.

References & further reading

Further reading on this topic

These sources provide broader context; they are not presented as citations for every statement in this entry.

1. Advanced characterization techniques for solid state lithium battery research

   Yuxuan Xiang, Xia Li, Yongqiang Cheng, Xueliang Sun, Yong Yang · Materials Today · 2020

   Topic background · X-ray, solid-state NMR and neutron methods in solid-state battery research.