Battery knowledge · Materials analysis and post-mortem

Focused ion beam SEM

A scanning electron microscope paired with an ion beam that mills material away at a chosen spot. It cuts clean cross-sections through particles and coatings, lifts out thin slices for TEM, and by alternately milling and imaging rebuilds an electrode’s microstructure in 3D for porosity and tortuosity.

Abbreviation
FIB-SEM
Also called
focused ion beam, FIB, plasma FIB, serial sectioning

Example

Materials analysis and post-mortem: an example situation

Surface and bulk measurements may find different compositions in the same electrode without contradiction.

Read Focused ion beam SEM alongside Porosity in this context. The fraction of a layer’s volume that is empty space. In a lithium-ion electrode the pores — roughly 20–35 % of the volume after calendering — are filled with electrolyte, which carries ions to the particles.

Use in Lemonergy

Connect results with scale and specimen preparation.

This is a reference concept. No executable Lemonergy block has been verified for this term.

References & further reading

Further reading on this topic

These sources provide broader context; they are not presented as citations for every statement in this entry.

  1. Advanced characterization techniques for solid state lithium battery research

    Yuxuan Xiang, Xia Li, Yongqiang Cheng, Xueliang Sun, Yong Yang · Materials Today · 2020

    Topic background · X-ray, solid-state NMR and neutron methods in solid-state battery research.