Energy-dispersive X-ray spectroscopy

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Binder migration

Binder carried to the top of the coating by evaporating solvent during fast drying, leaving the foil interface binder-poor. The result is weak adhesion and higher resistance; it is controlled by drying profile and slurry formulation.

Scanning electron microscopy

Imaging a surface with a focused electron beam at magnifications far beyond light microscopy. In battery work it shows particle cracking, plated lithium and coating morphology; cross-sections show the layer structure of an electrode.

Transition-metal dissolution

Manganese, nickel or cobalt ions leaching from the positive electrode into the electrolyte, especially at high voltage and temperature or when HF is present. They migrate to the negative electrode and poison the SEI there, accelerating lithium loss.

Transmission electron microscopy

Imaging by passing an electron beam through a specimen thinner than about 100 nm, fine enough to resolve rows of atoms. It reveals the nanometre-thick rock-salt layer that forms on aged nickel-rich particles, the structure of SEI and CEI, and cracks within particles; specimens are usually thinned with a focused ion beam.

X-ray fluorescence

Exciting a sample with X-rays and reading the characteristic X-rays each element re-emits — a fast, largely non-destructive composition measurement. It checks nickel, manganese and cobalt ratios, coating loading and black-mass grades, and finds transition metals deposited on aged anodes, but it cannot detect lithium.

References & further reading

Further reading on this topic

These sources provide broader context; they are not presented as citations for every statement in this entry.

1. Advanced characterization techniques for solid state lithium battery research

   Yuxuan Xiang, Xia Li, Yongqiang Cheng, Xueliang Sun, Yong Yang · Materials Today · 2020

   Topic background · X-ray, solid-state NMR and neutron methods in solid-state battery research.